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B/R
Instrument 800 - High Efficiency Micro Distillation
This
high efficiency, micro fractional distillation system is an ideal
tool for automatically purifying or analyzing a wide range of materials
where only very small amounts of sample are available. Common applications
include:
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Teaching Aid |
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Crude
Oil Distillation |
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Petroleum
Distillation |
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Close
Boiling Point Separations |
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High
Purity Fractional Distillation |
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Essential
Oil Purification |
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Vacuum
Distillation |
Features:
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All Glass and Teflon Components |
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30
Theoretical Plates Distillation Column (maximum at atmosphere) |
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10,
15, 25 ml boiler capacities |
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Automatic
and Manually Operated Distillation Systems |
This micro
spinning band distillation system is a very powerful tool for separating
close boiling components. O-ring seals allow joints to be "grease
free". Vacuum distillations can be carried out to as low as
0.1 mm Hg. Special glassware allows receivers to be changed without
interrupting the vacuum regulation.
Specifications:
| Column |
Length |
Diameter |
Max.
Plates |
Standard
Flask Sizes |
| 800
Micro Spinning Band |
20
cm |
7mm |
30
(Teflon Band) |
10,
15, and 25ml |
Automation
and Accessories:
All our distillation equipment is available in fully automatic or
manually operated models. Manually operated distillation systems
are inexpensive and simple to operate. Automatic models are microprocessor
controlled. All the distillation functions are fully automated to
make the distillation process easy and efficient from beginning
to end.

M690
Microprocessor Controller
The microprocessor
minimizes the amount of operator time required for each distillation.
Call up your stored program from one of 19 available memory locations
and let the microprocessor perform the distillation. Each program
can store up to eight distillation fractions. Each fraction has
programmable open and close temperature cut points, heat rates,
and equilibration times. Programmable shut down at the end of the
distillation run. The microprocessor allows easy editing of each
of the parameters while the distillation is in progress.
VAC-1000
Vacuum Regulation System
Materials that
have very high boiling points or are subject to thermal degradation
should be distilled at reduced pressures. The VAC-1000 is a complete,
stand alone vacuum system that can provide regulated vacuum to any
distillation system. It features a 5 decade pressure sensor, proportional
control valve, vacuum manifold/trap, 2 stage mechanical pump, all
mounted on a roll around cart for easy maneuverability in the laboratory.
The VAC-1000 can be used with automated or manually operated columns.
Fraction Collectors
Five place
fraction collectors are available. Receiver sizes are 2 ml. The
fraction collector is a convenient way to collect fractions without
having to change receivers.

Mounting
The 800 micro
still is mounted in an open frame support structure. The open frame
allows easy access to all areas of the distillation column. The
distillation column, microprocessor and fraction collectors are
mounted in the framework.
Recirculating Baths
The distillation
equipment requires cooling for the column condenser. Cold tap water
can be easily attached to the column's condenser. B/R offers heated
and refrigerated recirculating baths for more precise control of
the condenser temperature.
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